測(cè)定石膏粉的結(jié)晶水含量

Determination of crystal water content of gypsum powder

濟(jì)南石膏粉是一種結(jié)晶混合物，含有生石膏、半水合物和硬石膏（超煅石膏）。在炒制過(guò)程中，在火下會(huì)出現(xiàn)石膏，或者火太大、炒制時(shí)間過(guò)長(zhǎng)會(huì)出現(xiàn)無(wú)水石膏，影響石膏的凝固時(shí)間，影響生產(chǎn)的正常使用。有時(shí)由于石膏粉放置時(shí)間過(guò)長(zhǎng)受潮，也會(huì)影響正常使用。

Jinan gypsum powder is a crystalline mixture containing raw gypsum, hemihydrate and anhydrite (super calcined gypsum). In the process of frying, gypsum will appear under the fire, or anhydrous gypsum will appear if the fire is too large and the frying time is too long, which will affect the setting time of gypsum and the normal use of production. Sometimes the gypsum powder will be affected by damp due to its long storage time, which will also affect its normal use.

據(jù)經(jīng)驗(yàn)和資料介紹，石膏粉的好壞可以通過(guò)測(cè)定結(jié)晶水的含量來(lái)判斷。一般合格石膏粉的結(jié)晶水含量在4.5-5.5%之間。如果石膏粉的結(jié)晶水含量遠(yuǎn)低于這個(gè)標(biāo)準(zhǔn)值，說(shuō)明石膏粉過(guò)燒，注塑時(shí)凝固時(shí)間過(guò)長(zhǎng)甚至不凝固；石膏粉的結(jié)晶水含量遠(yuǎn)高于這個(gè)標(biāo)準(zhǔn)值，說(shuō)明石膏粉在火或潮濕下，注塑成型時(shí)凝固時(shí)間短。以上兩種情況的石膏粉不合格，不能用于生產(chǎn)。

According to experience and information, the quality of gypsum powder can be judged by measuring the content of crystal water. Generally, the crystal water content of qualified gypsum powder is between 4.5-5.5%. If the crystal water content of gypsum powder is far lower than the standard value, it indicates that the gypsum powder is burned, and the solidification time is too long or even does not solidify during injection molding; The crystal water content of gypsum powder is much higher than this standard value, which indicates that the solidification time of gypsum powder during injection molding is short under fire or humidity. The gypsum powder in the above two cases is unqualified and cannot be used in production.

石膏粉結(jié)晶水含量的檢測(cè)方法如下：精密稱取試樣質(zhì)量G（一般為2-5g），經(jīng)40℃干燥后冷卻至室溫，置于鉑坩堝（或瓷坩堝）中)恒重。準(zhǔn)確稱量其質(zhì)量為G1；在230±5℃下燒2h，取出轉(zhuǎn)移到干燥器中，冷卻至室溫后稱重質(zhì)量為G2，其結(jié)晶水百分比為（Gt-G2）/GX100%。

The test method for the crystal water content of gypsum powder is as follows: accurately weigh the sample mass g (generally 2-5g), dry it at 40 ℃, cool it to room temperature, and place it in a platinum crucible (or porcelain crucible) for constant weight. Accurately weigh its mass to G1; Burn it at 230 ± 5 ℃ for 2h, take it out and transfer it to a dryer. After cooling to room temperature, the weight is G2, and the percentage of crystal water is (gt-g2) /gx100%.

測(cè)定石膏粉的凝結(jié)時(shí)間

Determination of setting time of gypsum powder

濟(jì)南石膏粉的凝固時(shí)間包括初凝時(shí)間和終凝時(shí)間。標(biāo)準(zhǔn)稠度下，一般初凝時(shí)間不小于6min，終凝時(shí)間不大于25min。使用中初凝時(shí)間過(guò)短，小于6min，說(shuō)明石膏粉未熟，或潮濕中含有生石，影響注塑操作，表現(xiàn)為生產(chǎn)時(shí)注桶，延誤生產(chǎn);如果終凝時(shí)間過(guò)長(zhǎng)，遠(yuǎn)大于25tnin，說(shuō)明石膏在油炸過(guò)程中過(guò)燒，其中含有過(guò)燒石膏，在注塑成型時(shí)容易漏漿，甚至石膏漿也會(huì)漏漿。不凝固，影響生產(chǎn)。

The setting time of Jinan gypsum powder includes initial setting time and final setting time. Under standard consistency, generally, the initial setting time is not less than 6min, and the final setting time is not more than 25min. The initial setting time in use is too short, less than 6min, indicating that the gypsum powder is not mature, or there is green stone in the wet, which affects the injection molding operation, which is manifested as barrel injection during production, delaying production; If the final setting time is too long, which is far greater than 25tnin, it indicates that the gypsum is burned during the frying process, which contains burned gypsum. It is easy to leak slurry during injection molding, and even the gypsum slurry will leak slurry. No solidification, affecting production.

兩種情況下的石膏粉都不能用于生產(chǎn)。因此，凝固時(shí)間的確定可以判斷石膏粉的質(zhì)量，也可以決定石膏粉能否用于生產(chǎn)。簡(jiǎn)單的測(cè)量方法如下

In both cases, gypsum powder cannot be used for production. Therefore, the determination of setting time can determine the quality of gypsum powder and whether gypsum powder can be used in production. Simple measurement methods are as follows

(1)按制得的膏體與水的比例稱取100ml水所需的石膏粉試樣，將水倒入500ml容器中，1min內(nèi)將試樣均勻?yàn)⑷胨校o置30s，快速攪拌30s，立即將石膏漿倒入放置在玻璃板上的銅管中，然后將銅管慢慢垂直向上提起20mm，使石膏漿壓平成約5mm厚的試餅；

(1) Weigh the gypsum powder sample required for 100ml of water according to the ratio of the prepared paste to water, pour the water into a 500ml container, evenly sprinkle the sample into the water within 1min, stand for 30s, quickly stir for 30s, immediately pour the gypsum slurry into the copper tube placed on the glass plate, and then slowly lift the copper tube vertically upward for 20mm to flatten the gypsum slurry into a test cake about 5mm thick;

(2)用直徑約5nun的玻璃棒切試餅，每30s一次，每劃一次后用布擦拭玻璃棒。當(dāng)劃痕兩側(cè)的漿液剛剛不再合攏時(shí)，即為初凝狀態(tài)。試樣放入水中至初凝的時(shí)間間隔為初凝時(shí)間；

(2) Cut the test cake with a glass rod with a diameter of about 5nun, once every 30s, and wipe the glass rod with a cloth after each scratch. When the slurry on both sides of the scratch is no longer closed, it is in the initial setting state. The time interval between putting the sample into water and initial setting is the initial setting time;

(3)初凝后的試餅，用大拇指以約50N的力連續(xù)按壓，間隔15s，當(dāng)壓印邊緣無(wú)水分時(shí)，即為終凝。終凝時(shí)間是從樣品開(kāi)始入水到終凝的時(shí)間間隔。

(3) For the test cake after initial setting, use your thumb to press it continuously with a force of about 50N at an interval of 15s. When there is no water at the impression edge, it is the final setting. The final setting time is the time interval from the beginning of the sample entering the water to the final setting.

根據(jù)檢測(cè)結(jié)果與質(zhì)量標(biāo)準(zhǔn)或石膏粉在正常規(guī)模化生產(chǎn)中的凝固時(shí)間值的比較，可以判斷石膏粉的質(zhì)量是否可以用于生產(chǎn)。

According to the comparison between the test results and the quality standards or the setting time of gypsum powder in the normal large-scale production, we can judge whether the quality of gypsum powder can be used in production.

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